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直读光谱仪使用过程中的注意事项
1
One
试料激发与计算机操作时,鉴于安全,计算机的操作和激发试样,必须由一个人操作到底。激发试样前先将试样放好才能使用计算机的操作指令。在激发岗位操作时要注意听声音,试料放置不好,有漏气时,激发声音则不正常。每个试样,必须激发二次以上,计算机操作时,应记下炉号,次数和钢种,并要记录操作者的姓名。检查激发放电斑点,凝聚放电是好的,扩散放电(白点)是不好的。检查激发点的位置上是否有微小裂纹,气孔和砂眼,激发点有无重叠等,提供给数据处理工作时做重要的参考。
With the computer operation to stimulate sample, in view of safety, the operation of the computer and the excited sample, must be operated by a single person in the end. Before the sample is excited, the sample is put in order to use the operating instructions of the computer. In the excitation of post operation should pay attention to listen to the sound, the sample placed well, leakage, stimulate the sound is not normal. Each sample must be excite more than two times. When the computer is operated, the number of the furnace, the number of times and the steel should be recorded, and the name of the operator should be recorded. It is not good to check the excitation discharge spots, and the condensed discharge is good, and the diffusion discharge (white spot) is not good. Whether the micro crack check the position of the excitation point, and stomatal trachoma, excitation point has no overlap, to the data processing work as an important reference.
2
Two
数据处理操作时,须着重指出的是,在验证分析试样的时间,也要激发接近含量的标钢,以便证明仪器是在正常的工作。数据的选择和取舍要稳重,要考虑多方面的因素,如铁值的变化,其它元素的变化,插入铝量,激发斑点、激发声音等,有时需要重磨试样分析验证,有时候需要多次激发来验证。分析数据,一律以标钢含量为准,以控制标钢的正负偏差为准。每次新换氩气后,工作曲线必须重新标准化,当瓶内压力降到15个大气压时,需要更换新氩气;如果在工作过程中发现激发斑点呈白点状,也应另换一瓶新氩气。
When data processing is done, we must point out that when testing the time of the sample, we should also stimulate the standard steel close to the content so as to prove that the instrument is working normally. The choice and trade-off of data must be steady. There are many factors to consider, such as the change of iron value, the change of other elements, the amount of aluminum inserted, the excitation of spots, and the excitation of sound. Sometimes, we need to re sharpen and analyze samples, and sometimes we need multiple excitations to verify. The analysis of the data is based on the standard steel content to control the positive and negative deviations of the standard steel. Every time the new argon is changed, the working curve must be re normalized. When the pressure in the bottle drops to 15 atmospheres, new argon should be replaced. If the spot is white like, it should be replaced with another bottle of new argon.

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